PREPARATION OF TiN FILMS BY N_2 ASSISTED Xe~+ ION BEAM ENHANCED DEPOSITION AND THEIR MECHANICAL PROPERTIES

A new method for preparation of hard TiN films has been developed by using electronbeam evaporation-deposition of Ti and bombardment with 40 keV Xe~+ ion beam ina N_2 gas environment.The synthesized TiN films were superior to PVD and CVDones in respects of improved adhesion to substrate and low preparing temperature.Theyexhibited good wear resistance and high hardness up to 2200 kg/mm~2.Some industrialapplications have been reported.     

图像中的文本定位技术研究综述

介绍了图像中文本定位技术的研究现状,依据定位所利用的特征进行分类,分析了其中几种典型算法,并对文本定位算法的性能评价标准进行了深入讨论。     

基于Web services的WebGISVisA体系结构研究与实现*

针对目前网络地理信息系统体系结构难以实现Internet环境下的异构空间信息的互操作问题,深入分析其主要原因,在对现有网络地理信息系统的三层体系结构进行深入分析的基础上,提出一种基于Web services的网络地理信息系统体系结构(Web-based geographical information services visualization architecture,WebGISVisA).WebGISVisA体系结构通过Web services对各个地理信息系统组件进行包装,实现各个组件的跨平台操作,从技术上使得客户端和服务端达到了负载平衡,完成了WebGIS三维的虚拟现实,实现了在Internet下空间数据互操作和跨平台的功能,最大限度地达到数据共享.     

工业大麻中大麻二酚的后脱羧协同超临界萃取

目的:提供一种后脱羧协同超临界萃取制备大麻二酚(CBD)的方法.方法:工业大麻花叶预处理及干燥后进行二氧化碳超临界萃取.萃取温度为20～50℃,压力为10～30 MPa,二氧化碳流量为500～900 kg·h-1,时间为1～4 h.萃取物经过前处理后进行脱羧.脱羧后的CBD粗油通过分子蒸馏及高效液相色谱纯化,真空浓缩,结晶,制得高纯度CBD晶体.结果:与脱羧前相比,脱羧后CBDA含量明显降低,转化率在75％以上.制得的成品CBD晶体纯度均在99.7％以上,平均质量分数为99.86％.结论:脱羧协同二氧化碳超临界萃取可提高CBD提取效率、降低生产成本,适合工业化大规模生产.     

主变方向过流保护拒动原因分析

针对某变电站主变10 kV方向过流保护拒动情况,从保护原理、现场接线、定值设置等方面,分析电流互感器的极性选择及方向元件控制字的设置对短路功率方向的影响,提出规范二次接线、合理设置控制字等防止保护拒动和误动的相关措施,确保方向过流保护动作的正确性.     

Formation of Proto-Kranz in C3 Rice Induced by Spike-Stalk Injection Method

Introduction of C4 photosynthetic traits into C3 crops is an important strategy for improving photosynthetic capacity and productivity. Here, we report the research results of a variant line of sorghum–rice (SR) plant with big panicle and high spikelet density by introducing sorghum genome DNA into rice by spike-stalk injection. The whole-genome resequencing showed that a few sorghum genes could be integrated into the rice genome. Gene expression was confirmed for two C4 photosynthetic enzymes containing pyruvate, orthophosphate dikinase and phosphoenolpyruvate carboxykinase. Exogenous sorghum DNA integration induced a series of key traits associated with the C4 pathway called “proto-Kranz” anatomy, including leaf thickness, bundle sheath number and size, and chloroplast size in bundle sheath cells. Significantly, transgenic plants exhibited enhanced photosynthetic capacity resulting from both photosynthetic CO₂-concentrating effect and improved energy balance, which led to an increase in carbohydrate levels and productivity. Furthermore, such rice plant exhibited delayed leaf senescence. In summary, this study provides a proof for the feasibility of inducing the transition from C3 leaf anatomy to proto-Kranz by spike-stalk injection to achieve efficient photosynthesis and increase productivity.     

Facile Fabrication of Poly(vinyl alcohol)/Polyquaternium-10 (PVA/PQ-10) Anion Exchange Membrane with Semi-Interpenetrating Network

Anion exchange membranes (AEMs) are one of the core components of AEM fuel cells. A series of poly(vinyl alcohol)/polyquaternium-10 (PVA/PQ-10) AEMs with semi-interpenetrating networks (s-IPNs) are prepared by a simple solution-casting method using glutaraldehyde (GA) as a cross-linking agent. Subsequently, the prepared PVA/PQ-10 cross-linked membranes are characterized by Fourier transform infrared spectroscopy, scanning electron microscopy, thermogravimetric analysis, mechanical analysis, water uptake and swelling ratio tests, ion exchange capacity (IEC) tests, ionic conductivity measurements, and oxidative/alkaline stability tests. The effects of the mass ratio of PVA and PQ-10 and the amount of cross-linking agent GA on the performance of the PVA/PQ-10 cross-linked membranes are systematically explored. The results show that the cross-linked PVA/PQ-10 AEMs have high IEC and low water uptake and swelling ratio, and its maximum ionic conductivity can reach 79.37 mS cm^–1 at 80 °C. In addition, the PVA/PQ-10 cross-linked membrane has good oxidative and alkaline stability under optimal preparation conditions. These results may provide valuable insights toward more effective scheme designs and new, simple preparation methods for AEMs with s-IPN structures.     

NiAl金属间化合物的热爆合成过程研究

以Al粉和Ni粉为主要原料，采用自蔓延高温合成技术，制备Ni—Al基金属间化合物。绘制了热爆反应曲线、描述了热爆反应的过程，分析了热爆反应机理及产物的显微组织特征，研究了热爆反应的边界条件以及各种反应参数对热爆反应的影响。研究结果表明，升温速率和颗粒尺寸对热爆反应均有不同程度的影响。提高升温速率、减小颗粒尺寸均可缩短热爆反应的起始时间，降低热爆反应的起始温度。初步确定了反应起始温度低于Ni—Al系的最低共晶温度（640℃），Ni—A1系的热爆反应是由固一固扩散反应引发的，Ni-32Al的反应产物为单相、均一的NiAl相。     

LD7铝合金时效工艺的研究

通过试验系统地研究了ＬＤ７铝合金的单级和两级时效工艺。结果表明，与传统的单级时效相比，两级时效在不降低室温强度，硬度的前提下，可显著提高合金的电导率及高温性能。